The method of catalytic synthesis of benzyl cinnamate with hexadecyl trimethyl ammonium chloride as phase transfer catalyst is studied. The factors influencing the reaction, such as amount of catalyst used, reaction temperature and time, molar ratio of sodium cinnamate to benzyl chloride are investigated.

  • 以十六烷基三甲基氯化铵为相转移催化剂催化合成肉桂酸苄酯,考察了催化剂、温度、时间和物料配比等因素对反应的影响。
  • 来源:互联网摘选更新时间:2025-01-20 11:54:07

  • 重点词汇
  • theart.这个;指已提到或易领会到的人或事物;指独一无二的、正常的或不言而喻的人或事物;用以泛指;与形容词连用,指事物或统称的人;用于姓氏的复数形式前,指家庭或夫妇;(指特定用途的事物)足够,恰好;每,一;当前的,本,此;(重读,表示所指的为知名或重要的人或事物)
  • such as像, 例如;譬如;诸如;
  • catalyticadj.接触反应的;起催化作用的;
  • influencingadj.影响的;
  • amountn. 量,数量;总额;本利之和;全部效果,全部含义;
  • synthesisn.综合;<化>合成;综合体;综合推理;
  • methodn.方法;有条不紊;
  • catalystn.<化>触媒,催化剂;〈比喻〉触发因素;促进因素;〈口〉有感染力的人;
  • reactionn.反应(能力);不良反应;化学反应;抗拒,反对;
  • sodiumn.<化>钠(11号元素,符号 Na);
  • ammonium chloriden.氯化铵,卤砂;
  • 相关例句
2、

The result shows that, hexadecyl trimethyl ammonium chloride is an effective catalyst and under the optimal condition, 86.0% yield of benzyl cinnamate can be obtained.

实验结果表明,十六烷基三甲基氯化铵是一种有效的催化剂,在最佳反应条件下,产物收率可达86.0%。

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3、

The result shows that tetrabutylammonium bromide was an effective catalyst and the optimum conditions of preparation were determined with yield of benzyl cinnamate 85.3%.

实验结果表明:四丁基溴化铵是一个有效的催化剂,在最适宜的条件下,产物收率可达85.3%。

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4、

Microwave assisted synthesis of benzyl cinnamate catalyzed by NKC-9 macroporous resin

微波协同NKC-9大孔树脂催化合成肉桂酸苄酯

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5、

New process for synthesis of benzyl cinnamate

肉桂酸苄酯的合成新工艺

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6、

This experiment filtrates the benzyl penicillin strain with high yield by mutagenesis the benzyl penicillin strain No. 232 which available and used for the manufacture.

本试验通过用化学诱变剂对现有青霉素生产菌株232~进行诱变育种,筛选高产菌株。

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7、

Treatment with benzyl-penicillin are effective. Mutagenesis breeding of benzyl penicillin strain

青霉素治疗有效,未发现不良反应。青霉素产生菌的诱变育种

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8、

Benzyl penicillin potassium and other twenty-four antibiotic drugs were recognized using neural networks.

运用神经网络识别青霉素钾等24种抗生素药物的红外光谱。

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9、

This paper described the mechanisms of synthesis of benzyl acetate by tetranbutylammonium bromide in the presence of phase transfer catalyst, and such factors as temperature, time are also discussed.

该文描述了相转移催化剂存在时合成醋酸苄酯的机理,对反应温度、反应时间等因素也进行了讨论。

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10、

Benzyl Triphenyl Phosphonium Bromide;

苄基三苯基溴化磷;

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12、

The reaction of tosylate or benzyl bromide containing stopper with 4,4 ′-bipyridine was carried out under solvent-free.

通过固相熔融的方法,使4,4′-联吡啶与磺酸酯或苄溴进行反应。

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13、

Penicillin G potassium salt(ⅰ) was reacted with p-nitro benzyl bromide to produce the 4-nitrobenzyl ester of penicillin G acid(ⅱ).

以青霉素G钾盐Ⅰ为原料,与对硝基溴化苄反应生成青霉素G的对硝基苄酯Ⅱ。

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14、

Benzoyl cyanide was synthesized by the reaction of sodium cyanide with benzoyl chloride in a polar compounds as a catalyst with the yield of 72%.

在催化剂存在下,以固体氰化钠和苯甲酰氯为原料合成苯甲酰氰,研究了反应条件对收率的影响。优化条件下收率达72%(以苯甲酰氯计)。

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15、

The chloro group on benzene was shown to lower the biodegradability. STUDY ON THE THERMOKINETICS FOR NUCLEOPHILIC SUBSTITUTION REACTIONS OF BENZOYL CHLORIDE

苯环上氯取代会降低化合物的生物可降解性苯甲酰氯亲核取代反应的热动力学研究

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16、

The reaction of benzotrichloride and chloroacetic acid to form chloroacetyl chloride and benzoyl chloride in the presence of catalyst was studied.

研究了三氯甲苯和氯乙酸在催化剂存在下反应生成氯乙酰氯和苯甲酰氯的工艺条件。

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17、

The title compound has been prepared from the reaction of fluorescein and benzoyl chloride. Its crystal and molecular structure is determined by single crystal X-ray diffraction.

以荧光素和苯甲酰氯为原料制备了荧光素二苯甲酰酯,并用X射线单晶衍射法测定了晶体和分子结构。

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18、

It is based on phenol benzoate which is made from benzoyl chloride and phenol through rearrangement and etherification.

它主要由苯甲酰氯和苯酚制备苯甲酸苯酯,然后重排、醚化所得。

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19、

METHODS The intermediate 1 was synthesized via the friedel-crafts reaction between chlorobenzene and benzoyl chloride.

方法以氯苯和苯甲酰氯为原料,进行傅克酰化反应,合成出第一个反应中间体;

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20、

In this paper the synthetic methods and properties of benzoyl chloride are introduced, and its downstream products and its application are stated.

叙述了苯甲酰氯的性质、合成工艺路线、实验室和工业制法,产品规格及其分析方法。并对其深加工产品及其应用进行了概述。

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